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https://hdl.handle.net/10356/105703| Title: | Preparation and chiral separation of a novel immobilized cellulose-based chiral stationary phase in high-performance liquid chromatography | Authors: | Zhang, Zhen Bin Peng, G. M. Wu, S. Q. Fang, Z. L. Wu, S. S. Ng, S. C. Zhang, Wei-Guang Fan, Jun Zheng, Sheng-Run |
Keywords: | DRNTU::Engineering::Chemical engineering | Issue Date: | 2012 | Source: | Peng, G. M., Wu, S. Q., Fang, Z. L., Zhang, W. G., Zhang, B.Z., Fan, J., et al. (2012). Preparation and chiral separation of a novel immobilized cellulose-based chiral stationary phase in high-performance liquid chromatography. Journal of chromatographic science, 50(6), 516-522. | Series/Report no.: | Journal of chromatographic science | Abstract: | The chiral selector 6-azido-2, 3-di(p-chlorophenylcarbamoylated) cellulose was synthesized and further chemically immobilized onto 5-μm amino functionalized spherical porous silica gel. It was used as chiral stationary phase in high-performance liquid chromatography. Thirty racemates were successfully separated into enantiomers in either normal phase mode or reversed-phase mode. Good reproducibility and stability of the chiral stationary phase have been demonstrated. | URI: | https://hdl.handle.net/10356/105703 http://hdl.handle.net/10220/17956 |
DOI: | 10.1093/chromsci/bms047 | Rights: | © 2012 The Authors (published by Oxford University Press). This paper was published in Journal of Chromatographic Science and is made available as an electronic reprint (preprint) with permission of Oxford University Press. The paper can be found at the following official DOI: [http://dx.doi.org/10.1093/chromsci/bms047]. One print or electronic copy may be made for personal use only. Systematic or multiple reproduction, distribution to multiple locations via electronic or other means, duplication of any material in this paper for a fee or for commercial purposes, or modification of the content of the paper is prohibited and is subject to penalties under law | Fulltext Permission: | open | Fulltext Availability: | With Fulltext |
| Appears in Collections: | SCBE Journal Articles |
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