Please use this identifier to cite or link to this item: https://hdl.handle.net/10356/95329
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dc.contributor.authorBoey, Freddy Yin Chiangen
dc.contributor.authorDong, Zhilien
dc.contributor.authorSun, X. L.en
dc.contributor.authorTok, Alfred Iing Yoongen
dc.date.accessioned2013-03-14T09:02:35Zen
dc.date.accessioned2019-12-06T19:12:42Z-
dc.date.available2013-03-14T09:02:35Zen
dc.date.available2019-12-06T19:12:42Z-
dc.date.copyright2007en
dc.date.issued2007en
dc.identifier.citationTok, A. I. Y., Boey, F. Y. C., Dong, Z., & Sun, X. L. (2007). Hydrothermal synthesis of CeO2 nano-particles. Journal of Materials Processing Technology, 190(1-3), 217-222.en
dc.identifier.issn0924-0136en
dc.identifier.urihttps://hdl.handle.net/10356/95329-
dc.identifier.urihttp://hdl.handle.net/10220/9404en
dc.description.abstractNano-crystalline particles of CeO2 have been synthesized via a low temperature hydrothermal synthesis process. Two types of precursors were studied—cerium hydroxide and ceria acetate. The precursors were adjusted to a basic (pH 10) and acidic (pH 4) medium before hydrothermal treatment at various durations of 6, 12, 18, and 24 h at 250 °C using a Teflon-lined hydrothermal bomb. The synthesized samples were characterized using DTA/TGA, XRD and TEM. Based on the characterization results, both precursor systems produced crystalline ceria nano-particles after 6 h of hydrothermal synthesis at 250 °C. The average crystallite sizes were 6 and 15 nm for the hydroxide and acetate system, respectively. The acetate precursor system appeared to produce better particles in terms of crystallinity and morphology. Based on the DTA/TGA analysis, hydrothermal synthesis had been effective in reducing the amount of intermediate products. With increasing hydrothermal treatment duration of up to 24 h, the samples did not exhibit a remarkable improvement in properties. The synthesized nano-particles were subsequently heat treated at 500 and 1000 °C for 2 h. After the heat treatment, enhanced crystallinity and growth in crystallite size was observed, but particles appeared more agglomerated.en
dc.language.isoenen
dc.relation.ispartofseriesJournal of materials processing technologyen
dc.rights© 2007 Elsevier B.V. This is the author created version of a work that has been peer reviewed and accepted for publication by Journal of Materials Processing Technology, Elsevier B.V. It incorporates referee’s comments but changes resulting from the publishing process, such as copyediting, structural formatting, may not be reflected in this document. The published version is available at: [http://dx.doi.org/10.1016/j.jmatprotec.2007.02.042].en
dc.subjectDRNTU::Science::Physics::Heat and thermodynamicsen
dc.titleHydrothermal synthesis of CeO2 nano-particlesen
dc.typeJournal Articleen
dc.contributor.schoolSchool of Materials Science and Engineeringen
dc.identifier.doihttp://dx.doi.org/10.1016/j.jmatprotec.2007.02.042en
dc.description.versionAccepted versionen
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